取代芳酰胺基丙基杂氮硅三环化合物的合成

Synthesis of Substituted Aroyl Aminopropyl Silatranes

通过氨丙基杂氮硅三环与取代苯甲酰氯的酰基化反应 ,合成了 7种取代芳酰胺基丙基杂氮硅三环化合物 ,产率 4 9%～ 83% ;用1HNMR和IR等方法对其结构进行了鉴定 ,并初步探讨了反应条件。

s:Seven kinds of substituted aroyl-aminopropyl silatranes were synthesized by the acylation of γ-aminopropyl silatrane and substituted benzoyl chlorides,with a yield of 49%～83%. The structures of the compounds were identified by means of IR and 1H NMR and the conditions of the reaction were approached.