2,5-二甲氧基-4-丙巯基-β-硝基苯乙烯的合成方法改进

Synthesis of 2,5-dimethoxy-β-nitro-4-propylthio-styrene

报道了 2 ,5 二甲氧基 4 丙巯基 β 硝基苯乙烯的合成。以 2 ,5 二甲氧基苯甲醛为起始原料 ,经溴代、丙硫醇取代及与硝基甲烷缩合反应 ,合成了 2 ,5 二甲氧基 4 丙巯基 β 硝基苯乙烯。

This paper reported the synthesis of 2,5 dimethoxy β nitro 4 propylthio styrene.2,5 Dimethoxy β nitro 4 propylthiostyrene was synthesized via bromination,substitution with 1 propanethiol and condensation with MeNO 2 using 2,5 dimethoxybenzaldehyde as the raw material.