微波辐射条件下4-烷氧基苯乙酸的合成

The Synthesis of 4-Alkyloxyphenyiacetic Acid Under Microwave Irradiation

作者采用常压微波辐射的方法 ,以 4 烷氧基苯乙酮为原料 ,合成了一系列 4 烷氧基苯乙酸 .该法反应速度快 ,收率高 ,设备简单 。

A series of 4 alkyloxyphenylacetic acid were synthesized by the reaction of 4 alkyloxyacetophe none with sulfur and morpholine under microwave irradiation. The method has the advantage of high yield,sh ort reaction time and simple equipment. All the compounds were characterized by IR, 1HNMR,and MS.