毛细管气相色谱/质谱法测定东川芎中的挥发性成分

Determination of volatile components in Cnidium offcinale Makino by capillary GC/MS/MSD

[目的 ]测定东川芎中的挥发性成分 .[方法 ]用正己烷萃取东川芎根中的挥发性成分 ,以毛细管气相色谱 /质谱 /计算机法测定其成分 .[结果 ]检出丁基酞内酯 (butylPhthalide)、1α 乙烯基 2 β 己烯 环丙烷 (cydopropane ,1 ethenyl 2 hexenyl ,[1,alpha ,2 ,beta])、苯甲醇 (benzenemethanol)、藁本内酯(ligustilide)、9,12 二烯十八酸甲酯 (9,12 octadecadienoicacid ,methylester)、11,14 二烯二十酸甲酯 (11,14 eicosadienoicacid ,methylester)等 6种挥发性成分 .

OBJECTIVE?To detect the volatile components in Cnidium offcinale Makino .?METHODS??The volatile components in Cnidium offcinale Makino were extracted with skellysolve B and detected by capillary GC/MS/MSD.?RESULTS??It was found that six volatile components of the butyl phthalide;cydopropane,1 ethenyl 2 hexenyl ,[1,alpha,2,beta],benzenemethanol,ligustilide,9,12 octadecadienoic acid,methyl ester,11,14 eicosadienoic acid,methyl ester.