摘要
由丙二酸酯和2—溴丁烷通过仲丁基丙二酸酯合成了3—甲基戊酸,并研究了影响3—甲基戊酸产率的因素,还对其光谱性质进行了测定。并对实验结果进行了讨论。
3—methyl pentanoie acid was synthesized from malonic ester and 2—bromobutane through intermediate sec—butylmatlonie ester.Factors which influenced the yeld of 3—methyl pentanoic acid were studied.The structure of 3—methyl pentanoic acid was identified by IR and ~1H NMR.
出处
《郑州大学学报(自然科学版)》
CAS
1991年第1期97-99,共3页
Journal of Zhengzhou University (Natural Science)
关键词
3-甲基戊酸
合成
食用
香料
3—methyl pentanoic acid
Malonic ester
Org.synthesis