2-叔丁氨甲基-2-硝基-l,3-丙二醇盐酸盐的合成与表征

Synthesis and Characterization of 2-tert-butylaminomethyl-2-nityl-1,3-propanediol hydrochloride

以3-叔丁基-5-羟甲基-5-硝基四氢-l,3-噁嗪为原料,以水为溶剂,经酸性水解合成了2-叔丁氨甲基-2-硝基-l,3-丙二醇盐酸盐,并对其结构进行了红外光谱、核磁共振波谱和元素分析表征。

2-Tert-butylaminamethyl-2-nityl-1,3-propanediol hydrochloride was synthesized with 3-tert-butyl-5-nitro-tetrahydro-1,3（4H）-oxazine as materials, water as solvent by acid hydrolysis, the product was characterized by IR, HNMR, CNMR and element analysis. The result shows that the structure characteristics of product is accorded with 2-tert-butylaminamethyl-2-nityl-1,3-propanediol hydrochloride.