期刊文献+

4,4'-二异丁基-2,2'-联吡啶的合成及表征

Synthesis and Characterization of 4,4'-diisobutyl-2,2'-bipyridine
下载PDF
导出
摘要 以4,4'-二甲基-2,2'-联吡啶为原料,设计出一种简便、有效、安全的4,4'-二异丁基-2,2'-联吡啶的合成方法,简化了实验操作,提高了目标产物的收率,为后续用4,4'-二异丁基-2,2'-联吡啶作为配体的化合物在分子磁体方面的研究打下了坚实的基础。 4,4'- diisobutyl-2,2'-bipyridine was synthesized from 4,4'-dimethyl 2,2'-bipyridine. This method simplified the experimental operation and improved the yield of target product. It laid a solid foundation for subsequent with 4,4'-diisobutyl-2,2'-bipyridine as ligands in the research of molecular magnetism.
作者 严安平 文君
出处 《广东化工》 CAS 2014年第16期37-37,51,共2页 Guangdong Chemical Industry
基金 贵州省自然科学基金项目(No:2012076) 贵阳市科技计划项目(筑科合同[2012207]15号)
关键词 4 4'-二异丁基-2 2'-联吡啶 合成方法 结构表征 4,4'- diisobutyl-2,2'-bipyridine synthesis structural characterization
  • 相关文献

参考文献6

  • 1Bruce D,McCall J,Richter M.Effects of Electron Withdrawing and Donating Groups on the Efficiency of Tris(2,2'-Bipyridyl) Ruthenium(Ⅱ)/Trin-Propylamine Electrochemilum inescence[J].Analyst,2002,127:125-128.
  • 2Maruyama K,Mishima Y,Minagawa K,et al.DNA Sensor with a Dipyridophena-zine Complex of Osmium(Ⅱ) as an Electrochemical Probe[J].Anal.Chem.,2002,74(15):3698-3703.
  • 3Paul D B,Zheng C,A listair J G,et al.Fridrich Szemes and TrevorWear,Anion Recognition by Novel Ruthenium(Ⅱ) BipyridylCalyx Arene Receptor Molecules[J].J.Chem.Soc.Chem.Commun,1994,10:1269-1271.
  • 4Gratzel Z M,Fraser D M.Glucose Oxidase Mediation by Soluble and Immobilized Electroactive Detergents[J].Biosens Bioelectron,1996,11(3):305-315.
  • 5Masayuki N,Yoshihiro S,Hiroki O,et al.Controlled Intramolecular Electron Transfers in Cyanide-Bridged Molecular Squares by Chemical Modifications and External Stimuli[J].J.Am.Chem.Soc,2011,133,3592-3600.
  • 6Bos K D,Noltes J G.Improved Synthesis of 4,4'-Disubstituted-2,2'-Bipyridines[J].Syn.commun,1979,9(6):497-504.

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部