期刊文献+

皮革中邻苯二甲酸酯的快速筛选——离子迁移谱法 被引量:3

Screening of Plasticizers in Leather Products by Ion Mobility Spectroscopy
下载PDF
导出
摘要 建立了一种筛选皮革中邻苯二甲酸酯类增塑剂的方法。以丙酮为萃取溶剂,在40℃下微波萃取30min,萃取液经离子迁移谱检测,可实现对6种邻苯二甲酸酯的快速筛选。该方法简便快速,灵敏度高,各邻苯二甲酸酯检测低限在7~180mg,kg之间,满足欧盟REACH法规限量检测要求。 A screening method for the determination of phthalates plasticizers in leather using ion mobility spectroscopy is presented in this paper. The samples were extracted at 40℃ for 30 min by ultrasonic using acetone as the extracting solvent. The extract was analyzed by ion mobility spectroscopy, which enables the fast screening of 6 phthalates. The detection limit of each phthalate is between 7-180 mg/kg, which meets the determination requirement of REACH regulation.
出处 《西部皮革》 2014年第18期35-38,共4页 West Leather
基金 江苏出入境检验检疫局科研项目(2013KJ21)
关键词 皮革 邻苯二甲酸酯 离子迁移谱 筛选 REACH法规 leather phthalates ion mobility spectroscopy screening REACH regulation
  • 相关文献

参考文献5

二级参考文献140

  • 1王海龙,魏开华.离子淌度质谱及其理论研究进展[J].军事医学科学院院刊,2004,28(6):585-589. 被引量:4
  • 2许峰,王海龙,关亚风.离子迁移谱研究进展[J].化学进展,2005,17(3):514-522. 被引量:40
  • 3李金香,武波涛,王兴军.离子迁移谱技术发展趋势和应用前景[J].舰船科学技术,2006,28(2):13-15. 被引量:12
  • 4[1]Giuseppe L,Antonio DV,Marika M,et al.Phthalate exposure and male infertility[J].Toxicology,2006,226:90-98.
  • 5[2]Hurst CH,Waxman DJ.Activation of PPARalpha and PPARgamma by environmental phthalate monoesters[J].Toxicol Sci,2003,74:297-308.
  • 6[3]Bility MT,Thompson JT,McKee RH,et al.Activation of mouse and human peroxisome proliferator-activated receptors (PPARs) by phthalate monoesters[J].Toxicol Sci,2004,82:170-182.
  • 7[4]Corton JC,Lapinskas PJ.Peroxisome proliferator-activated receptors:mediators of phthalate ester-induced effects in the male reproductive tract[J].Toxicol Sci,2005,83:4-17.
  • 8[5]Kold JT,Scheike T,Ducot B,et al.How would a decline in sperm concentration over time influence the probability of pregnancy[J].Epidemiology,2004,15:458-465.
  • 9[6]Foster PM,Gray E,Leffers H,et al.Disruption of reproductive development in male rat offspring following in utero exposure to phthalate esters[J].Int J Androl,2006,29:140-147.
  • 10[7]Lehmann KP,Phillips S,Sar M,et al.Dose-dependent alterations in gene expression and testosterone synthesis in the fetal testes of male rats exposed to di (n-butyl) phthalate[J].Toxicol Sci,2004,81:60-68.

共引文献189

同被引文献77

  • 1GB/T20388-2006,纺织品邻苯二甲酸酯的测定[S].
  • 2GB/T 21928—2008食品塑料包装材料中邻苯二甲酸酯的测定[S].
  • 3SN/T1779-2006塑料血袋中邻苯二甲酸酯类增塑剂的测定气相色谱串联质谱法[S].
  • 4GB/T22048-2008玩具及儿童用品聚氯乙烯塑料中邻苯二甲酸酯增塑剂的测定[S].
  • 5SN/T 2037-2007与食品接触的塑料成型品中邻苯二甲酸酯类增塑剂迁移量的测定气相色谱质谱联用法[S].
  • 6GB/T28599-2012化妆品中邻苯二甲酸酯类物质的测定[S].
  • 7ISO8124-6-2014玩具安全第6部分玩具和儿童产品中的特定邻苯二甲酸酯类[S].
  • 8SN/T3620-2013玩具材料中邻苯二甲酸二异丁酯的测定GC-MS法[S].
  • 9GB/T30646-2014涂料中邻苯二甲酸酯含量的测定气相色谱质谱联用法[S].
  • 10GB/T24168-2009纺织染整助剂产品中邻苯二甲酸酯的测定[S].

引证文献3

二级引证文献24

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部