摘要
目的:研究杜仲叶中的化学成分.方法:采用各种柱色谱方法分离纯化,通过理化常数测定和光谱分析鉴定化合物的结构.结果:从杜仲叶中分离并鉴定了10个化合物,分别为牛蒡子苷(1),表松脂素(2),二羟基脱氢二松柏醇(3),3,4-二羟基-苯甲酸(4),D-核糖-1,4-内酯(5),L-核糖-1,4-内酯(6),尿苷(7),α-D-吡喃葡萄糖基-(1→3)-α-D-吡喃葡萄糖基-(1→2)-β-D-呋喃果糖苷(8),杜仲醇(9),1-脱氧杜仲醇(10).结论:化合物1,4~8为首次从杜仲叶中分离得到.
Objective:To investigate the chemical constituents of Eucommiae Folium.Method:The compounds were isolated and purified byvarious column chromatography techniques,the chemical structureswere elucidated by physiochemical properties and spectral analysis.Result:Ten compounds were isolated and identified asarctiin (1),epipinoresinol (2),dihydroxydehydrodiconiferyl (3),3,4-dihydroxy-benzoic acid (4),D-ribono-1,4-1actone (5),L-ribono-1,4-1actone (6),uridine (7),β-D-glucopyranosyl-(1→3)-α-D-glucopyranosyl-(1 → 2)-β-D-fructofuranoside (8),eucommiol (9),1-deoxyeucommiol (10).Conclusion:Compounds 1,4-8 were isolated from this plantfor the first time.
出处
《中国实验方剂学杂志》
CAS
北大核心
2014年第20期118-120,共3页
Chinese Journal of Experimental Traditional Medical Formulae
基金
国家自然科学基金项目(81160508)
"江西道地药材及特色中药资源杜仲研究"校级专项课题(ZX1020)
关键词
杜仲叶
化学成分
杜仲醇
Eucommiae Folium
chemical constituents
eucommiol