摘要
目的:研究彝族“黄药”的化学成分.方法:正相硅胶柱层析、葡聚糖凝胶Sephadex LH-20、制备薄层层析、反相制备色谱等手段分离纯化,根据其光谱数据进行结构鉴定.结果:从彝族黄药中分离鉴定出8个化合物,分别为liquiritigenin (1),β-sitosterol(2),kumatakenin(3),glycyrol(4),isoglycyrol(5),focosyl caffeate(6),inuchinenolide B(7),neogaillardin(8). 结论:其中化合物1,3-8为首次从该植物中分离得到.
Objective:To study the chemical constituents of Blumea balsamifera.Method:The compounds were isolated by various chromatographic techniques including Silica gel,Sephadex LH-20,preparative HPLC,and their structures were identified by physicochemical and spectral data.Result:Eight compounds were isolated from B.balsamifera,and their structures were identified as liquiritigenin (1),β-sitosterol (2),kumatakenin (3),glycyrol (4),isoglycyrol (5),focosyl caffeate (6),inuchinenolide B (7),neogaillardin (8).Conclusion:Compounds 1,3-8 were isolated from B.balsamifera for the first time.
出处
《中国实验方剂学杂志》
CAS
北大核心
2014年第21期106-108,共3页
Chinese Journal of Experimental Traditional Medical Formulae
基金
国家自然科学基金项目(81303308)
中国民族事务管理委员会科教司项目(10ZY09)
中央民族大学自主科研项目(1112KYQN42)
关键词
彝族“黄药”
艾纳香
化学成分
‘Huangyao’ in Yi nationality's medicine
Blumea balsamifera
chemical constituents