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含氟磺酰胺衍生物的合成与表征 被引量：1

Synthesis of Fluorine-containing Sulfonamide Derivatives
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摘要 文章通过三步反应合成了一个含氟磺酰胺衍生物。由2-氟苯胺与2-硝基-3-氟苯磺酰氯生成磺酰胺,然后再分别进行取代和还原反应得到N-(2-氟苯基)-2,2-二甲基-4-氧-2,3,4,9-四氢-1H-咔唑-8-磺酰胺。所合成的化合物通过了1H NMR、MS等光谱方法进行表征。 In this thesis, a sulfonamide derivative was synthesized by a three-step reaction. 2-fluoroaniline was turned into Sulfonamide by sulfonylation with 3-fluro-2-nitrobenzenesulfonyl chloride, and then through substitution and reduction reaction to give N-（2-fluorophenyl）-2,2-dimethyl-4-oxo-2,3,4,9-tetrahydro-lH- carbazole-8-sulfonamide, which was characterized by 1 HNMR and MS spectroscopy.
作者 荣方 王勃 吴德林
机构地区 池州学院材料与化学工程系
出处 《广东化工》 CAS 2014年第20期13-14,25,共3页 Guangdong Chemical Industry
基金 2013年国家大学生创新训练计划项目
关键词 磺酰胺 还原 合成 表征 sulfbnamide reduction synthesis characterized
分类号 TQ [化学工程]
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参考文献9

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二级参考文献35

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广东化工
2014年 第20期

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