摘要
本文对2-氨基-9,9-二甲基芴的合成工艺进行研究。由芴为起始原料,通过选择不同的合成方法,改变反应条件,确定最佳的合成工艺。反应产物通过高效液相色谱检测其纯度,通过核磁共振确定结构,所得产物均与目标化合物相符。
2- amino- 9,9- dimethylfluorene is a promising photovoltaic material. However,this type of material in China is still in the preliminary stage. In this paper,the methods of synthesis of 2- amino- 9,9- dimethylfluorene are especially studied. The fluorene used as the starting material for the reaction,the different ideas of synthesis chosen and some reaction conditions changed,the optimum conditions for the synthesis of 2- amino- 9,9- dimethylfluorene have been obtained. The product has been detected through high- performance liquid chromatography to determine the purity,and through nuclear magnetic resonance to determine the structure of the products. The product obtained is in line with the goal of the product.
出处
《江西化工》
2014年第3期140-142,共3页
Jiangxi Chemical Industry