摘要
[目的]将活性三七与普通干燥三七不同部位进行质量特征对比研究,为建立活性三七药材质量标准研究提供依据。[方法]通过显微结构、红外光谱、重金属残留、各皂苷含量、有效成分溶出率及醇溶浸出物含量等分析测试手段,同时对活性三七与普通干燥三七进行定性鉴别与定量研究,分析其有效成分和特征结构的变化。[结果]显微结构有差异;红外光谱特征区相同,指纹区有差异;活性三七重金属残留低于普通干燥三七;活性三七各皂苷含量、有效成分溶出量及醇溶浸出物均高于普通干燥三七。[结论]三七药材经过冷冻干燥处理后,具有明显的特征结构,质量优于普通干燥三七。
[Objective] To contrast the quality characteristics of Panax notoginseng treated with freeze drying and ordinary drying process,and establish the criterion of quality control for active Panax notoginseng.[Method] Quantitative research and qualitative identification of Panax notoginseng treated with different drying process were performed including micro-structure,FT-IR,heavy metal residue,the saponins content,the effective ingredient dissolution rate and the alcohol soluble extract content.[Result] There were obvious differences of micro-structure for the various of drying-treatment ; FT-IR spectrum were almost the same expect the fingerprint region ; heavy metal residues in Panax notoginseng treated with freeze drying were lower than that treated with ordinary drying; Saponin content,the alcohol soluble extract content and dissolubility effective components of freeze drying samples were significantly higher than the ordinary sample.[Conclusion] Panax notoginseng has obvious characteristics of the structure after freeze drying process and has some advantages over the ordinary dry Panax notoginseng.
出处
《安徽农业科学》
CAS
2014年第35期12457-12460,12471,共5页
Journal of Anhui Agricultural Sciences
基金
云南省人才培养项目(KKSY201326118)
昆明理工大学分析测试中心基金(20140681)
关键词
三七
显微结构
红外光谱
含量测定
溶出度
Panax notoginseng
Microstructure
FT-IR
Content determination
Dissolution