摘要
用溶剂热法,在油胺溶剂中,160℃加热反应12h成功合成了CdS:Mn纳米晶体。并对油相中合成的材料进行了功能化修饰,用巯基乙酸对材料进行了包裹。借助X射线衍射分析、傅里叶红外光谱、荧光谱图等测试方法对材料进行了表征,XRD数据表明,合成的CdS:Mn晶体PDF#为80-0019。IR数据显示,在CdS:Mn材料上成功修饰上了羧酸(-COOH)。CdS:Mn晶体修饰前后主要发射峰从527nm蓝移至489nm。
CdS：Mn quantum dots were synthesized by using solvothermal method in olcylamine at 160℃ for 12 h. The as-prepared CdS：Mn crystals were investigated by X-ray diffraction, Fourier transform infrared spectroscopy and flurescence spectroscopy. The powder X-ray diffraction （XRD） showed that thc PDF of CdS：Mn crystals was 80-0019. IR absorption spectra showed that the carboxyl group （-COOH） is on the surface of CdS：Mn crystals. From the fluorescence spcctra The results showed that the main peak of nanoparticles of modified CdS：Mn was blueshifted from 527 nm to 489 nm.
出处
《广东化工》
CAS
2015年第2期47-47,62,共2页
Guangdong Chemical Industry
关键词
CDS
MN
油胺
溶剂热法
CdS
Mn
oleylamine
solvothermal method
