摘要
以氯化钠和硫酸铵为原料,采用正交设计法对氯化铵的制备条件进行了优化。实验结果表明:在物料比为21,冰浴冷却时间为20 min,蒸发水量为45%,冷却温度为35℃的条件下,单次结晶氯化铵的产率和纯度明显提高。
An experimental program was designed for preparing ammonium chloride from sodium chloride and ammonium sulfate based on the orthogonal design. The optimum conditions were determined as follows： material ratio 2：1, cooling time 20 min and temperature 35 ℃,water evaporation 45%. Under above conditions, the productivity and pure of ammonium chloride could be improved dramatically.
出处
《当代化工》
CAS
2015年第1期39-40,4,共3页
Contemporary Chemical Industry
关键词
氯化铵
转化法
正交设计
Ammonium chloride
Transformation
Orthogonal design
