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含Ni磁性介孔碳的制备及其结构表征 被引量:2

Synthesis and Characterization of Ni doped Mesoporous Carbon Materials
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摘要 采用一步法得到含Ni磁性介孔碳(Ni O/C).通过X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)、氮气吸脱附(BET)、拉曼分析、饱和磁化强度等测试对材料进行表征.研究发现,所制备的磁性Ni O/C材料具有介孔结构,可以很好地分散在水溶液中,且有高的磁性能,能通过外加磁场简单快速地进行磁性分离.该材料可以快速、高效吸附水溶液中的离子液体1-甲基-3-丁基咪唑氯盐([Bmim]Cl). Ni magnetic mesoporous carbon materials was synthesized by one step method. This material was characterized by XRD,SEM,TEM,Nitrogen adsorption-desorption,magnetic measurements and Raman spectra. The results show that the magnetic Ni O / C composite material can be well dispersed in aqueous solution,and exhibit excellent superparamagnetic behaviors. After adsorption,it could be readily separated from solution by applying an external magnetic field. This material can quickly and effective adsorb[Bmim]Cl ionic liquid form aqueous solution.
机构地区 哈尔滨师范大学
出处 《哈尔滨师范大学自然科学学报》 CAS 2015年第1期117-119,共3页 Natural Science Journal of Harbin Normal University
关键词 磁性介孔碳 结构表征 吸附 Mesoporous carbon Characterization Adsorption
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