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4,4'-二[N-(芘-1-基亚烃基)胺芳基]-2,2'-双噻唑的合成 被引量：1

Synthesis of 4,4'-Bis[( N-( pyren-1-ylmethylene) amino-aryl) ]-2,2'-bithiazole
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摘要 以硝基苯乙酮为原料,经α-溴代、缩合和还原3步反应制得4,4'-二氨芳基-2,2'-双噻唑(3a,3c,3e);3a,3c和3e分别与酰基芘经缩合反应合成了6个新型的希夫碱——4,4'-二[N-(芘-1-基亚烃基)胺芳基]-2,2'-双噻唑(5a^5f),其结构经1H NMR,FT-IR和元素分析表征。5a^5f的熔点均>300℃。 4,4＇-Bis（am/noaryl）-2,2＇-bithiazole（3a, 3c, 3e） were prepared by a three-step reaction of α-bmmination, condensation and reduction from nitro-substitute acetophenone. Six novel Schiff bases, 4,4＇-his [ （ N-（pyren-l-ylmethylene） aminoaryl ） ] -2,2＇-bithiazole （ 5a - 5f）, were synthesized by the condensaton reaction of 3a, 3e, 3e with acyl pyrene, respectively. The structures were characterized by 1H NMR, FT-IR and elemental analysis. The melting point of 5a - 5f were above 300 ℃.
作者 石玉芳 王桂林 孙金鱼 赵明根
机构地区 忻州师范学院化学系
出处 《合成化学》 CAS CSCD 2015年第3期231-234,248,共5页 Chinese Journal of Synthetic Chemistry
基金 忻州师范学院重点学科专项课题资助项目(XK201205) 忻州师范学院青年基金资助项目(201201)
关键词 芘衍生物 4 4-'二[N-(芘-1-基亚烃基)胺芳基]-2 2'-双噻唑 希夫碱 合成 pyrene derivate 4, 4＇-bis [ （ N-（ pyren-l-ylmethylene ） aminoaryl ） ]-2, 2＇-bithiazole Schiff base synthesis
分类号 O625.63 [理学—有机化学] O626.25 [理学—有机化学]
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