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白皮杉醇的简便合成

Convenient Synthesis of Piceatannol
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摘要 报道了一种白皮杉醇(E-5)的简便合成方法。以3,5-二羟基苯乙酸为原料,经Perkin缩合和脱羧异构化反应合成了E-5,总收率55%,其结构经1H NMR,IR和ESI-MS确认。 A convenient route for synthesizing piceatannol （E-5） was reported. E-5 was synthesized by a two-step reaction of Perkin condensation and decarboxylation-isomerization from 3,5-dihydroxy ben- zene acetic acid in overall yield of 55%. The structure was confirmed by 1H NMR, IR and ESI-MS.
作者 肖春芬 邹永
机构地区 广东岭南职业技术学院药学院 中国科学院广州化学研究所
出处 《合成化学》 CAS CSCD 2015年第3期252-254,共3页 Chinese Journal of Synthetic Chemistry
基金 广东岭南职业技术学院科学研究项目(KB201304)
关键词 白皮杉醇 Perkin缩合 脱羧异构化 合成 piceatannol Perkin condensation decarboxylation-isomerization synthesis
分类号 O625.31 [理学—有机化学]
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参考文献16

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二级参考文献9

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共引文献11

合成化学
2015年 第3期

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