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6-乙酰基-1,1-双二茂铁基丁烷与格氏试剂的反应及其产物的研究

Studies on the reaction of 6-acetyl-1, 1-bisferrocenylbutane with grignard reagent
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摘要 通过6-乙酰基-1,1-双二茂铁基丁烷与甲基格氏试剂和苯基格氏试剂反应,得到4种新的反应产物,并利用元素分析,红外光谱,核磁共振氢谱等测试手段对各反应产物进行了表征。通过实验确定了最佳反应原料比例,并对两种格氏试剂的反应及其产物进行了讨论。 Four new compounds were obtained from the reaction of 6-acetyl-1,1-bisferrocenylhutane with methyl grignard reagent and phenyl grignard reagent. These new compounds were characterized by IR spectrum, elemental analysis, 1HNMR spectra . The best reaction condition was confirmed and the reactions of these two kinds of gri- gnard reagent were discussed further more.
出处 《精细与专用化学品》 CAS 2014年第11期32-35,共4页 Fine and Specialty Chemicals
基金 内蒙古自然科学基金资助项目(200711020204)
关键词 6-乙酰基-1 1-双二茂铁基丁烷 格氏试剂 表征 6-acetyl-l,l-bisferrocenylbutane grignard reagent characterization
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参考文献7

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