摘要
通过6-乙酰基-1,1-双二茂铁基丁烷与甲基格氏试剂和苯基格氏试剂反应,得到4种新的反应产物,并利用元素分析,红外光谱,核磁共振氢谱等测试手段对各反应产物进行了表征。通过实验确定了最佳反应原料比例,并对两种格氏试剂的反应及其产物进行了讨论。
Four new compounds were obtained from the reaction of 6-acetyl-1,1-bisferrocenylhutane with methyl grignard reagent and phenyl grignard reagent. These new compounds were characterized by IR spectrum, elemental analysis, 1HNMR spectra . The best reaction condition was confirmed and the reactions of these two kinds of gri- gnard reagent were discussed further more.
出处
《精细与专用化学品》
CAS
2014年第11期32-35,共4页
Fine and Specialty Chemicals
基金
内蒙古自然科学基金资助项目(200711020204)