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混合气体比例对脉冲直流PCVD制备TiN/TiSiN涂层的影响

Influence of Mixed Gas Ratio to Ti N / Ti Si N Coating Prepared by Pulsed DC of PCVD System
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摘要 采用工业用直流脉冲等离子体增强化学气相沉积PCVD技术在硅烷、氢气和氮气的混合气氛下成功制备了Ti Si N涂层,重点讨论了混合气体比例对薄膜性能的影响。结果表明:当混合气体中H2∶N2为4∶1、硅烷流量为2sccm时,Ti N/Ti Si N涂层中硅含量为8.01at%,此时,获得此工艺薄膜的最高硬度为28GPa。 The Ti Si N coating was successfully prepared by the use of PCVD technology what the industrial use of pulsed DC plasma enhanced chemical vapor deposition of,in the conditions of mixed atmosphere of silane,hydrogen and nitrogen. This paper main discussed the influence of mixed gas ratio on the properties of the films. The result shows that:when the H2∶ N2 gas mixture is 4∶1,silane flow rate is 2sccm,the silicon content of Ti N / Ti Si N coating is 8. 01at%,at this same time,the highest hardness acquired is 28 GPa.
出处 《工具技术》 北大核心 2015年第4期16-17,共2页 Tool Engineering
基金 国家科技重大专项"复杂数控刀具创新能力平台建设"(2012ZX0412021)
关键词 PCVD TI N/Ti SI N 成膜速率 硬度 膜成分 PCVD Ti N / Ti Si N film forming rate hardness film composition
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  • 1李戈扬,王公耀,吴亮,李鹏兴,张流强,郑永铭.双靶反应溅射Ti-B-N复合膜的研制[J].上海交通大学学报,1997,31(4):108-113. 被引量:9
  • 2Veprek S, Nesladek P, Niederhofer A, et al. Recent progress in the superhard nanocrystalline composites:towards their industrialization and understanding of the origin of the superhardness[J]. Surf Coat Tech, 1998, 108-109:138-147.
  • 3Veprek S. The search of novel superhard materials[J]. J Vac Sci Tech A, 1999, 17(5):2401-2420.
  • 4Holubar P, Jilek M, Sima M. Nanocomposite nc-TiAlSiN and nc-TiN-BN coatings: their applications on substrates made of cemented carbide and results of cutting tests[J]. Surf Coat Tech, 1999, 120-121:184-188.
  • 5Mitterer C, Mayrhofer P H, Beschliesser M, et al. Microstructure and properties of nanocomposite Ti-B-N and Ti-B-C coatings[J]. Surf Coat Tech, 1999, 120-121:405-411.
  • 6Vaz F, Rebouta L, Goudeau P, et al. Characterisation of Ti1-xSixNy nanocomposite films[J]. Surf Coat Tech,1999, 120-121:166-172.
  • 7Diserens M, patscheider J, Levy F. Improving the properties of titanium nitride by incorporation of silicon[J]. Surf Coat Tech, 1998, 108-109:241-246.
  • 8Diserens M, Patscheider J, Levy F. Mechanical properties and oxidation resistance of nanocomposite TiN-SiNx physical-vapor-deposited thin films[J]. Surf Coat Tech, 1999, 120-121:158-165.
  • 9Nesladek P, Veprek S. Superhard nanocrystalline composites with hardness of diamond[J]. Phys Stat Sol A, 2000, 177(1):53-62.
  • 10Niederhofer A, Nesladek P, Mannling H D, et al. Structural properties, internal stress and thermal stability of nc-TiN/α-Si3N4, nc-TiN/TiSix and nc-(Ti1-yAlySix)N superhard nanocomposite coatings reaching the hardness of diamond[J]. Surf Coat Technol, 1999, 120-121:173-176.

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