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无溶剂无催化剂条件下合成betti碱

Catalyst-free Synthesis of Betti Bases under Solvent-free Conditions
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摘要 在无溶剂无催化剂条件下,无论是含有吸电子基团还是含有供电子基团的芳香醛都能与2-萘酚以及仲胺反应,短时间内以高产率生成氨基烷基萘酚。该方法实验操作简单,不需要使用催化剂和溶剂,减少了废物排放,降低了成本,是一种绿色合成氨基烷基萘酚的方法。 Aromatic aldehyde containing electron-donating and electron-withdrawing substituents was reacted with 2-naphthol and secondary amine to furnish aminoalkylnaphthols in short time with high yield under solvent-free conditions in the absence of catalyst. The advantages of these reactions were simplicity of the reaction procedure, simple work-up, catalyst-and solvent-free conditions, reducing the amount of waste, and lower cost. The present method provides a green route for synthesis of aminoalkylnaphthols.
作者 张婷 熊武鑫 丁文强 周忠强
机构地区 中南民族大学化学与材料科学学院
出处 《广州化工》 CAS 2015年第9期77-79,共3页 GuangZhou Chemical Industry
基金 中南民族大学2015年大学生创新创业训练计划项目(XCX15011)
关键词 betti碱 无溶剂 合成 betti base solvent-free synthesis
分类号 O621.3 [理学—有机化学]
  • 相关文献

参考文献9

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二级参考文献14

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广州化工
2015年 第9期

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