摘要
目的:完善薄荷水的质量控制方法。方法采用薄层色谱法鉴别薄荷水中的薄荷素油,用气相色谱法测定薄荷水中薄荷脑的含量。结果薄层色谱法鉴别专属性强;气相色谱法中,薄荷脑线性范围为5.0∽80.0μg/ml(r=0.9999),平均回收率为103.16%,RSD为1.81%。结论该法操作简便,结果准确,灵敏度高,重复性好,可有效地控制薄荷水的质量。
Objective To consummate a method of quality control of peppermint water .Methods Thin layer chromatog-raphy was used for the identification of peppermint oil .Gas chromatography was used for the determination of mentholum . Results The identification of peppermint oil was highly specific by TLC .The linear range of mentholum was from 5 .0-80 .0 μg/ml ,r=0 .999 9 .The average recovery of mentholum was 103 .16% and RSD was 1 .81% .Conclusion These methods were easy to operate with accurate results ,which washigh sensitivity andgoodrepeatability .This quality standard could effective-ly control the quality of peppermint water .
出处
《药学实践杂志》
CAS
2015年第3期255-257,共3页
Journal of Pharmaceutical Practice
基金
军队医疗机构制剂标准提高科研专项重点课题(13ZJ01)
关键词
薄荷水
质量控制
薄层色谱法
气相色谱法
薄荷脑
peppermint water
quality standard
thin layer chromatography
gas chromatography
mentholum