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Boc保护氨基合成方法学的研究 被引量：3

Research of Synthetic Methodology of Boc-Protected Amino Groups
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摘要 对两种新颖的Boc保护氨基的绿色化学合成方法进行了全面比较和总结,找到了一些有用的规律,为以后的科研工作提供有价值的参考。 Two novel synthetic methods of green chemistry for boc - protected amino groups were compared and summarized comprehensively in this paper. Some useful rules were found, which provided valuable references for the future scientific research.
作者 娄绍霞 崔迎 赵倩倩
机构地区 天津渤海职业技术学院
出处 《山东化工》 CAS 2015年第11期59-60,共2页 Shandong Chemical Industry
关键词 Boc保护氨基 合成方法学 总结规律 boc - protected amino group synthetic methodology summary rule
分类号 TQ031.2 [化学工程]
  • 相关文献

参考文献13

  • 1Kocienski P J.Protecting Groups[M].New York:Georg Thieme Verlag,2000.
  • 2Sartori G.,Ballini R,Bigi F,et al.Protection(and deprotection)of functional groups in organic synthesis by heterogeneous catalysis[J].Chem Rev,2004,104(1):199-250.
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  • 7Guibe-Jampel E,Wakselman M.An easy preparation of the water-soluble t-butoxycarbonylating agent 1-boc-4-dimethylaminopyridinium tetrafluoroborate[J].Synthesis,1977(11):772.
  • 8Greene T W,Wuts P G M.Protecting group in organic synthesis[M].3rd ed.New York:John Wiley and Sons,1999.
  • 9Varala R,Nuvula S,Adapa S R.Molecular iodine-catalyzed facile procedure for N-boc protection of amines[J].J Org Chem,2006,71(21):8283-8286.
  • 10Chankeshwara S V,Chakraborti A K.Catalyst-free chemoselective N-tert-butyloxycarbonylation of amines in water[J].Org Lett,2006,8(15):3259-3262.

二级参考文献15

  • 1Lutz C, Lutz V, Knochel P. Enantioselective synthesis of 1,2 -, 1,3 - and 1,4 - aminoalcohols by the addition of dialkylzincs to 1,2 -, 1,3 - and 1,4 - aminoaldehydes [J]. Tetrahedron, 1998, 54(23) : 6385 -6402.
  • 2Guibe - Jampel E, Wakselman M. An easy preparation of the water - soluble t - butoxycarbonylating agent 1 - boc - 4 - dimethylaminopyridinium tetrafluoroborate [ J ]. Synthesis, 1977, (11) : 772.
  • 3Greene T W, Wuts P G M. Protecting Group in Organic Synthesis, 3rd ed. [M]. John Wiley and Sons: New York, 1999.
  • 4Varala R, Nuvula S, Adapa S R. Molecular iodine - cat- alyzed facile procedure for N - boc protection of amines [J].J. Org. Chem. 2006, 71(21): 8283-8286.
  • 5Chakraborti A K, Chankeshwara S V. HClO4 - SiO2 as a new, highly efficient, inexpensive and reusable catalyst for N - tert - butoxycarbonylation of amines[J]. Org. Biomol. Chem. , 2006, 4(14): 2769-2771.
  • 6Chankeshwara S V, Chakraborti A K. Catalyst -free chemoselective N - tert - butyloxycarbonylation of amines in water [J]. Org. Lett., 2006, 8(15): 3259-3262.
  • 7Heydari A, Khaksar S, Tajbakhsh M. 1,1,1,3,3,3 - Hexafluoroisopropanol: a recyclable organocatalyst for N - Boc protection of amines [J]. Synthesis, 2008, ( 19 ) 3126 - 3130.
  • 8Kocienski P J. Protecting Groups[ M ]. C, eorg Thieme Verlag: New York, 2000.
  • 9Sartori G, Ballini R, Bigi F., et al. Protection (and deprotection) of functional groups in organic synthesis by heterogeneous catalysis [ J ]. Chem. Rev. , 2004, 104 (1) : 199 -250.
  • 10Chakrabortl A K, Gulhane R. Zirconium(IV) chloride as a new, highly efficient, and reusable catalyst for acetyla- tion of phenols, thlols, amines, and alcohols under solvent -free conditions[J]. Synlett, 2004, (4) : 627 -630.

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山东化工
2015年 第11期

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