摘要
目的 建立舒筋活血丸中樟脑限量检查方法。方法 采用气相色谱法测定,色谱柱为DB-WAX石英毛细管柱（30 m×0.32 mm,0.25μm）,柱温为程序升温。结果 樟脑在浓度1.05~210.40μg·m L-1范围内,浓度与峰面积成线性（r=1.0）,平均加样回收率101.7%（n=9,RSD=1.2%）。结论 该方法简便、灵敏,结果准确,重复性好,适用于舒筋活血丸质量控制。
Objective To establish a method for limit test of camphor in Shujin Huoxue pills. Methods A DB-WAX （30 m×0. 32 mm,0. 25 μm） capillary column was used with a programmed temperature. Results The linear range of camphor was 1. 05-210. 00 μg·mL-1（r=1. 0）. The average recovery was 101. 7%（n=9, RSD=1. 2%）. Conclusion The proposed method is simple, sensitive, accurate and reproducible, which is suitable for quality control of Shujin Huoxue Pills.
出处
《医药导报》
CAS
2015年第7期950-952,共3页
Herald of Medicine
关键词
舒筋活血丸
樟脑
色谱法
气相
质量控制
Shujin Huoxue Pills
Camphor
Chromatography,gas
Quality control
