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几种典型羟基化多溴联苯醚和多溴联苯的合成、纯化及鉴定 被引量：1

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摘要 通过耦合、氧化和溴化等基本有机化学反应,合成并纯化了几种典型羟基多溴联苯醚和多溴联苯.通过C18半制备高效液相色谱柱对反应粗成品进行分离与纯化,以气相色谱-质谱和氢谱核磁共振对产物进行结构鉴定与表征.结果表明,合成制备的产物与目标物一致,纯度达99%以上.
作者 丁佳锋 苏勉 林坤德
机构地区 浙江工业大学生物与环境工程学院 厦门大学环境与生态学院
出处 《环境化学》 CAS CSCD 北大核心 2015年第7期1377-1379,共3页 Environmental Chemistry
基金 国家自然科学基金(21277124 21477115)资助
关键词 羟基多溴联苯醚 羟基多溴联苯 合成 提纯.
分类号 X830 [环境科学与工程—环境工程]
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参考文献5

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二级参考文献7

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共引文献1

同被引文献30

  • 1万云洋,杜予民.漆酶结构与催化机理[J].化学通报,2007,70(9):662-670. 被引量：48
  • 2Cynthia A de Wit.An overview of brominated flame retardants in the environment[J]. Chemosphere . 2002 (5)
  • 3Natalia N. Pozdnyakova,Janina Rodakiewicz-Nowak,Olga V. Turkovskaya,Jerzy Haber.Oxidative degradation of polyaromatic hydrocarbons catalyzed by blue laccase from Pleurotus ostreatus D1 in the presence of synthetic mediators[J]. Enzyme and Microbial Technology . 2006 (6)
  • 4Lillemor Asplund,Maria Athanasiadou,Andreas Sjodin,Ake Bergman,Hans Borjeson.Organohalogen substances in muscle, egg and blood from healthy Baltic salmon (Salmo salar) and Baltic salmon that produced offspring with the M74 syndrome. Ambio . 1999
  • 5Dingemans, Milou M L,Groot, Aart de,Kleef, Regina G D M van,Bergman, ?ke,Berg, Martin van den,Vijverberg, Henk P M,Westerink, Remco H S.??Hydroxylation Increases the Neurotoxic Potential of BDE-47 to Affect Exocytosis and Calcium Homeostasis in PC12 Cells(J)Environmental Health Perspectives . 2008 (5)
  • 6Inhibition of human placental aromatase activity by hydroxylated polybrominated diphenyl ethers (OH-PBDEs)(J)Toxicology and Applied Pharmacology . 2007 (1)
  • 7Jonathan Verreault,Geir W. Gabrielsen,Shaogang Chu,Derek C. G. Muir,Magnus Andersen,Ahmad Hamaed,Robert J. Letcher.Flame Retardants and Methoxylated and Hydroxylated Polybrominated Diphenyl Ethers in Two Norwegian Arctic Top Predators:? Glaucous Gulls and Polar Bears. Environmental Sciences . 2005
  • 8Steen, Peter O.,Grandbois, Matthew,Mcneill, Kristopher,Arnold, William A.Photochemical formation of halogenated dioxins from hydroxylated polybrominated diphenyl ethers (OH-PBDEs) and chlorinated derivatives (OH-PBCDEs). Environmental Sciences . 2009
  • 9Hooper K,McDonald T A.The PBDEs: an emerging environmental challenge and another reason for breast-milk monitoring programs. Journal of Environmental Health . 2000
  • 10Shigeyuki Takagi,Chiaki Shirota,Kazuko Sakaguchi,Jun Suzuki,Takumi Sue,Hiromitsu Nagasaka,Shin Hisamatsu,Shigenori Sonoki.??Exoenzymes of Trametes versicolor can metabolize coplanar PCB congeners and hydroxy PCB(J)Chemosphere . 2006 (9)

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环境化学
2015年 第7期

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