1,8-二氨基-3,6-二氧辛烷的合成研究

Study on Synthesis of 1,8-Diamino-3,6-dioxaoctane

以三乙二醇和溴化磷为原料,通过溴化反应和盖布瑞尔合成法制备1,8-二氨基-3,6-二氧辛烷。优化了1,8-二氨基-3,6-二氧辛烷的合成条件,通过FTIR和GC-MS对目标产物进行表征。

1,8-Diamino-3,6-dioxaoctane was prepared by bromination and the Gabriel synthesis of triethylene glycol and phosphorous tribromide, and the synthetic conditions were optimized. The structures of product was characterized by FTIR and GC-MS.