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无溶剂一锅法合成新型8-芳基-7,8-二氢-[1,3]二氧戊环并[4,5-g]喹啉-6(5H)-酮类化合物

Solvent-free Synthesis of Novel 8-Aryl-7,8-dihydro-[1,3]-dioxolo[4,5-g]quinolin-6( 5H)-one Compounds by One-pot Method
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摘要 采用微波辅助,经三组分（3,4-亚甲二氧基苯胺,2,2-二甲基-1,3-二氧六环-4,6-二酮和取代芳醛）无溶剂一锅法合成了10个新型的8-芳基-7,8-二氢-[1,3]二氧戊环并[4,5-g]喹啉-6（5H）-酮类化合物,产率75.7%~83.5%,其结构经1H NMR,FT-IR,ESI-MS和元素分析表征。 Ten novel 8-aryl-7,8-dihydro- [ 1,3 ] -dioxolo [ 4,5 -g ] quinolin-6 （ 5 H） -one compounds, in yield of 75.7 % - 83.5 %, were synthesized by one-pot method under solvent-free conditions, using 3,4-（methylenedioxy） aniline, 2,2-dimethyl-1,3-dioxane-4,6-dione and aldehydes as materials. The structures were characterized by ^1H NMR, FT-IR, ESI-MS and elemental analysis.
作者 吴晓霞
机构地区 南京晓庄学院生物化工与环境工程学院
出处 《合成化学》 CAS CSCD 2015年第9期861-864,共4页 Chinese Journal of Synthetic Chemistry
关键词 二氧戊环并[4 5-g]喹啉-6(5H)-酮 一锅法 无溶剂 合成 dioxolo [ 4,5-g ] quinolin-6 （5H） -one one-pot method solvent-free synthesis
分类号 O626.3 [理学—有机化学]
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参考文献11

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合成化学
2015年 第9期

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