六应丸中丁香酚的气相色谱测定法

GC GETERMINATION OF EUGENOL IN LIU YING WAN

中成药六应丸是由蟾酥、牛黄、冰片、丁香等药物组成,具有解毒、消炎、退肿、止痛等功效。本文探索了生药公丁香及成药六应丸中的丁香酚的气相色谱测定法,并比较了不同的提取过程对含量测定的影响。方法简便,准确。

A GC method for thedetermination of eugenol in crude medic-ine and its preparation Liuying Wan hasbeen proposed. Sample was treated withcelite-545-column. Analysis was carriedout on chromosorb WHP 80～100 mesh.Column packed with 3% polyglycol 20000,column temperature 160'C. For quantitiveanalysis octadecane was used as the inter-nal standard. This method is rapid, repreducible.and has been applied to the eugenolcontents in various samples.