期刊文献+

草酰二肼硝酸盐的制备及表征

Preparation and characterization of oxalylhydrazinium nitrates
下载PDF
导出
摘要 通过草酰二肼与硝酸溶液的质子化作用制备了草酰二肼一硝酸盐(OHN)和草酰二肼二硝酸盐(OHDN),产率均达95%。制备的产品用元素分析、红外、核磁对其结构进行了表征。性能测试表明OHN、OHDN的感度较低,且在75%相对湿度的环境中1周后吸湿率≤0.03%。 The oxalylhydrazinium nitrate(OHN) and oxalylhydrazinium dinitrate(OHDN) were prepared by protonation of oxalyldihydrazide and nitric acid solution,and the yields of the products all reach 95%.The structures of the prepared products were characterized by using elemental analysis,infrared spectrum,nuclear magnetic resonance.The performance testing shows that the sensitivity of OHN and OHDN is lower,the hygroscopicity in 75%relative humidity environment after one week is not more than 0.03%.
出处 《化学推进剂与高分子材料》 CAS 2015年第6期84-86,共3页 Chemical Propellants & Polymeric Materials
关键词 含能材料 草酰二肼硝酸盐 吸湿性 感度 energetic material oxalylhydrazinium nitrate hygroscopicity sensitivity
  • 相关文献

参考文献2

  • 1Fischer D, Klap6tke T M, Sterstorfer J. Oxalyhy- drazinium nitrate and dinitrate-Efficiency meets performance[J]. Journal of Energetic Materials, 2014, 32(1): 37-49.
  • 2Dewitt Ivan L, Pacanowsky Eugene. Oxalyl- dihydrazide compositions and use as a coolant gas generating process: US, 3839105[P]. 1974-10-01.

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部