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Determination of rhenium and osmium by ICP-MS for galena and sphalerite 被引量:1

Determination of rhenium and osmium by ICP-MS for galena and sphalerite
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摘要 Digestion with aqua regia in a Carius tube and separation of Re with anion exchange resin is commonly employed for Re–Os dating of molybdenite and pyrite.However, the recovery of Re is extremely low when this routine anion exchange method is applied to galena,causing difficulty in Re–Os dating of galena. In this study,we investigated the mechanism of Re loss during sample preparation and tested a revised procedure for Re–Os dating of galena and sphalerite. Digestion with aqua regia in a Carius tube and separation of Re with anion exchange resin is commonly employed for Re–Os dating of molybdenite and pyrite.However, the recovery of Re is extremely low when this routine anion exchange method is applied to galena,causing difficulty in Re–Os dating of galena. In this study,we investigated the mechanism of Re loss during sample preparation and tested a revised procedure for Re–Os dating of galena and sphalerite.
出处 《Acta Geochimica》 EI CAS CSCD 2016年第1期43-49,共7页 地球化学学报(英文)
基金 supported by the 12th Five-Year Plan Project of State Key Laboratory of Ore Deposit Geochemistry, Chinese Academy of Sciences (SKLODG-ZY125-09 SKLODGZY125-02) the National Natural Science Foundation of China (Nos. 41373064 41430315)
关键词 电感耦合等离子体质谱法 方铅矿 闪锌矿 测定 阴离子交换 离子交换法 树脂分离 制备过程 Galena Sphalerite Rhenium and osmium Anion exchange resin ICP-MS
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