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气相色谱—质谱联用技术分析藿香挥发油化学成分 被引量:13

Analysis of the Chemical Composition of Volatile Oil from Pogostemon cablin by GC-MS
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摘要 以湛江市遂溪县产藿香为研究对象,采用水蒸气蒸馏法提取藿香的挥发油成分,利用气相色谱—质谱联用技术结合程序升温保留指数进行定性分析,采用峰面积归一法进行定量分析.共分离出90种化学成分,鉴定了50种化合物,占挥发油总量的72.53%,主要成分有广霍香醇(24.88%)、δ-愈创木烯(16.05%)、α-广藿香烯(7.61%)、α-愈创木烯(7.36%)、丁香烯(3.63%)、β-广藿香烯(3.38%)、β-榄香烯(1.5%)和γ-丁香烯(1.0%). The essential oil of Pogostemon cablin from Suixi county, Zhanjiang City, Guang- dong Province was extracted by steam distillation and analyzed by gas chromatography- mass spectrometry (GC-MS). Meanwhile, the temperature-programmedretention index (PTRI) was employed to improve the accuracy of qualitative analysis.The relative concen- tration of each component was determined by peak area normalization. A total of 90 com- pounds were isolated, of which 50 compounds were chemically identified and accounted for 72.53% of the total peak area. The major components identified were Patchouli alcohol (24.88%) ,. delta.-Guaiene ( 16.05% ) ,. alpha.-Patchoulene (7.61%) , alpha.-Guaiene ( 7.36% ), Caryophyllene ( 3.63% ) ,. beta.-Patchoulene ( 3.38% ) ,. beta.-Elemene ( 1.5% ) and Isocarvophillene ( 1.0% ).
出处 《南华大学学报(自然科学版)》 2016年第1期77-81,共5页 Journal of University of South China:Science and Technology
基金 国家自然科学基金资助项目(11205085) 湖南省教育厅科学研究基金资助项目(12C0334)
关键词 藿香 挥发油 气相色谱-质谱 程序升温保留指数 Pogostemon cablin volatile oil gas chromatography-mass spectrometry ( GC-MS) temperature-programmedretention index (PTRI)
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