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QTRAP LC-MS/MS技术在污染事故快速定性中的应用 被引量：2

QTRAP LC-MS/MS:Rapid Qualitative Analysis Technique Used in a Pollution Incident Response
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摘要 采用液相色谱-四极杆/线性离子阱复合质谱(QTRAP LC-MS/MS)技术用于污染事故水样中未知农药的快速定性分析。由于QTRAP LC-MS/MS具有较好的灵敏度,样品无需前处理即可进样,大大提高了样品的分析速度。在某次污染事故水样定性分析工作中,该技术的应用非常快速地解决了污染源判定问题,为污染事故的应急处置提供了强有力的技术支撑。 QTRAP LC-MS/MS（liquid chromatography-quadrupole/ linear ion trap mass spectrometry） was used for qualitative analysis of unknown pesticide in a water pollution incident response. Because of the good sensitivity of QTRAP LC-MS/MS,the analysis can be done without sample pretreatment so that the qualitative analysis became time-saving.Application of this technique was quite efficient in tracing the pollution source in pollution incident,providing a strong technical support for the response to water pollution incidents.
作者 张蓓蓓 章勇 赵永刚
机构地区 国家环境保护地表水环境有机污染物监测分析重点实验室
出处 《环境科学与技术》 CAS CSCD 北大核心 2016年第4期79-82,101,共5页 Environmental Science & Technology
基金 2013年江苏省环境监测基金项目(1301、1305)
关键词 液相色谱-四极杆/线性离子阱复合质谱 快速定性 污染事故 QTRAP LC-MS/MS rapid qualitative analysis pollution incident
分类号 X832 [环境科学与工程—环境工程]
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参考文献16

  • 1Chen F,Zhang F,Yang N,et al.Simultaneous determination of 10 nucleosides and nucleobases in Antrodia camphorata using QTRAP LC-MS/MS[J].J Chromatogr Sci,2014,52(8):852-861.
  • 2Shen Y,Han C,Jiang Y,et al.Rapid quantification of four major bioactive alkaloids in Corydalis decumbens(Thunb.)Pers.by pressurised liquid extraction combined with liquid chromatography-triple quadrupole linear ion trap mass spectrometry[J].Talanta,2011,84(4):1026-1031.
  • 3Schaefer N,Peters B,Bregel D,et al.Can JWH-210 and JWH-122 be detected in adipose tissue four weeks after single oral drug administration to rats[J].Biomed Chromatogr,2014,28(8):1043-1047.
  • 4Zhou X,Cao S,Li X,et al.Simultaneous determination of18 preservative residues in vegetables by ultrahigh performance liquid chromatography coupled with triple quadrupole/linear ion trap mass spectrometry using a dispersive-SPE procedure[J].J Chromatogr B Analyt Technol Biomed Life Sci,2015,989(10):21-26.
  • 5Bertin J,Dury AY,Ke Y,et al.Accurate and sensitive liquid chromatography/tandem mass spectrometry simultaneous assay of seven steroids in monkey brain[J].Steroids,2015,16(98):37-48.
  • 6Michel D,Gaunt MC,Arnason T,et al.Development and validation of fast and simple flow injection analysis-tandem mass spectrometry(FIA-MS/MS)for the determination of metformin in dog serum[J].J Pharm Biomed Anal,2015,25(107):229-235.
  • 7于晓丽.QTrap在蔬菜农药残留量检测中的应用[J].食品工业,2014,35(7):245-247. 被引量：2
  • 8Gómez MJ,Martínez Bueno MJ,Agüera A,et al.Evaluation of ozone-based treatment processes for wastewater containing microcontaminants using LC-QTRAP-MS and LCTOF/MS[J].Water Sci Technol,2008:57(1):41-48.
  • 9Bueno MJ,Agüera A,Gómez MJ,et al.Application of liquid chromatography/quadrupole-linear ion trap mass spectrometry and time-of-flight mass spectrometry to the determination of pharmaceuticals and related contaminants in wastewater[J].Anal Chem,2007,79(24):9372-9384.
  • 10Lynch KL,Breaud A R,Vandenberghe H,et al.Performance evaluation of three liquid chromatography mass spectrometry methods for broad spectrum drug screening[J].Clin Chim Acta,2010,411(19/20):1474-1481.

二级参考文献22

  • 1张敬波,姜文凤,董振霖,赵守成,卫锋.气相色谱法同时测定玉米中12种三嗪类除草剂的残留量[J].色谱,2006,24(6):648-651. 被引量：36
  • 2[1]SKIDORE M W,PAULSON G D.et al.[J].J Pure and Application Chemistry,1998,70(7):1423-1447.
  • 3[2]Yu K,KROL J,BALOGH M.[J].J Analytical Chemistry,2003,75(16):4103-4112.
  • 4[3]SAUVAGE F L,SAINT-MORCOUX F,et al.[J].J Clinical Chemistry,2006,52(9):1735-1742.
  • 5Hager JW. A new linear ion trap mass spectrometer. Rapid Commun. Mass Spectrom., 2002,16:512～ 526
  • 6Hager JW, Yves Le Blanc JC. Product ion scanning using a Q - q - Qlinear ion trap (QTRAPTM) mass spectrometer. Rapid Commun. Mass Spectrom., 2003,17:1056 ～ 1064
  • 7Hager JW. Product ion spectral simplification using time- delayed fiagment ion capture with tandem linear ion traps. Rapid Commun. Mass Spectrom. ,2003,17:1389 ～ 1398
  • 8Hager JW, Yves Le Blanc JC. High- pefformance liquid chromatngraphy- tandem mass spectrometry with a new quadrupole/linear ion trap instrument. J. Chromatogr. A ,2003,1020:3 ～ 9
  • 9Hopfgartner G, Husser C and Zell M. Rapid screening and characterization of drug metabolites using a new quadrupole- linear ion trap mass spectrometerl. J. Mass Spectrom., 2003,38: 138～ 150
  • 10Xia YQ,Miller JD,Bakhtiar R, Franklin RB, Liu DQ. Use of a quadrupole linear ion trap mass spectrometer in metabolite identilication and bioanalysis. Rapid Commun. Mass SOectrom.,2003,17:1137 ～ 1145

共引文献18

同被引文献15

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二级引证文献11

环境科学与技术
2016年 第4期

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