摘要
研究强磁场对AZ31镁合金塑变能力和微观组织的作用,在3 T脉冲强磁场条件下对合金进行磁场耦合应力时的拉伸实验.采用电子背散射衍射、Ⅹ射线衍射和透射电镜分析等方法研究材料的微观组织.结果表明:与0 T拉伸试样相比,3 T拉伸试样抗拉强度和延伸率分别提高了2.2%和28.7%,说明将强磁场耦合作用于材料塑性变形过程时,能在不降低材料强度的同时提高镁合金的塑性变形能力,有助于同步改善材料强韧性.磁场作用机理主要表现为磁致塑性效应,计算表明主要合金相β(Mg_(17)Al_(12))为顺磁性,有助于发挥磁场作用效果.磁场提高了位错运动灵活性并促使位错增殖,晶界处位错堆积和应力集中促进了再结晶形成,晶粒发生细化,发挥细晶强韧化效果;同时磁场诱发塑性变形时的晶粒转动,新生成非基面取向的晶粒弱化了镁合金(0001)基面织构,该组织特征有助于提高材料的塑变能力.
As an h.c.p crystal structure with only a few limited slipping planes, the AZ31 magnesium alloy exhibits a bad plasticity in the presence of external stress. Due to its low density, advanced damping capacity and high ratio strength and rigidity, the magnesium alloy has gradually become the focused and potential structural and functional metallic material in the diverse fields of aerospace, aviation and vehicle transportation, electronic products, etc. Therefore, it is of great importance to improve the process ability of conventional magnetism alloy as AZ31. In the past decades many approaches have been proposed in order to improve the plastic deformation capability. Among these, the diverse physical fields are regarded as the effective methods to improve the comprehensive mechanical properties of metallic materials due to their peculiar heat, force and quantum effects together with the advantageous characteristics of low pollution and high efficiency. In the paper, on the basis of previous researches, a high pulsed magnetic field is introduced into the tensile test to study the influences of magnetic field on the plasticity and microstructure of AZ31 magnesium alloy in order to explore a novel way to enhance the plastic deformation capability of alloy. As for the current experiment,the tensile test of AZ31 magnesium alloy is carried out under the coupling action of high pulsed magnetic field and external stress. The test results are compared with those processed without magnetic field. Several advanced detection methods are utilized to investigate the microstructure including the electron back scattered diffraction, X-ray diffraction and transmission electron microscopy, etc. Besides, the first principle is utilized to calculate the magnetic properties of main precipitates β(Mg(17)Al(12)).The experimental results show that the tensile strength and elongation of the 3 T sample are increased by 2.2%and 28.7% in comparison to those of the 0 T sample. It highlights that when the high pulsed magnetic field is introduced into the plastic deformation process, the plasticity of the magnesium alloy can be improved without reducing the tensile strength of the material. The action mechanism of magnetic field is analyzed in detail and attributed to the magnetoplasticity effect. The calculation results on the basis of first principle show that the β(Mg(17)Al(12)) phase is paramagnetic,which is helpful for performing the effect of magnetic field. The magnetic field enhances the flexibility of the dislocation movement and facilitates the proliferation of the dislocation. The dislocation and stress concentrating at the grain boundaries accelerate the formation of recrystallization, which is of great importance to the sub-grain generation and grain refinement that is beneficial to exhibiting the fine grain strengthening and enhancing the strength and toughness of alloy. Meanwhile, during the peculiar tensile process, the magnetic field induces the grain rotation. The newborn fine grains along the non-basal face weaken the(0001) basal texture of magnesium alloy. The characteristic of the texture structure is helpful for improving the plastic deformation capacity of AZ31 alloy. The plastic deformation under high magnetic field is regarded as an advanced way to improve the plasticities of similar nonmagnetic metallic materials such as aluminum, titanium and copper alloys and their composites.
出处
《物理学报》
SCIE
EI
CAS
CSCD
北大核心
2016年第14期191-201,共11页
Acta Physica Sinica
基金
国家自然科学基金(批准号:51371091
51001054
51174099)
江苏省研究生科研创新计划(批准号:SJLX15_0490)资助的课题~~
关键词
强磁场
AZ31镁合金
织构
力学性能
high magnetic field
AZ31 magnesium alloy
texture
mechanical properties