摘要
采用对甲氧基苯胺为原料,将其制成重氮盐,然后在催化剂和表面活性剂的作用下和丙烯酸甲酯反应,合成了对甲氧基肉桂酸甲酯;通过熔点测定、质谱和气相色谱分析等手段对产物进行了结构表征和含量分析,并研究得到最佳工艺条件.
Methyl p-methoxy cinnamate was synthesized with p-Anisidine and Methyl acrylate, under the action of catalyst and surfactant. The structure was confirmed by melt point and MS with the content being analyzed by GC, and the optimum technological condition was determined.
出处
《河南科学》
2016年第9期1437-1439,共3页
Henan Science
基金
河南省科技厅高新类项目(142102210543)