摘要
采用微波热处理技术得到了Ti-Sn微米棒。采用XRD、SEM与EDS研究合成产物的组成相组成和微观形貌。研究结果表明,通过微波合成技术,采用2Ti/Sn/石墨粉体原料均得到大量Ti Sn微米棒。Ti-Sn微米棒的长度约5~10μm,宽度约2~3μm。石墨原料起到了诱发电弧放电的作用,从而促进Ti Sn柱状晶的形成。
The Ti-Sn micro-rod was synthesized by microwave heat treatment. The phase composition and microstructure of the samples were studied by XRD, SEM and EDS. The result showed that amounts of Ti-Sn microrods can be obtained by microwave synthesis from 2Ti/Sn/graphite. These micro-rods had a length of 5 ~ 10 μm and a width of 2 ~ 3 μm. Graphite played a role for inducing arc discharge and was benefits to synthesis of Ti-Sn micro-rod.
作者
梁宝岩
张旺玺
王艳芝
徐世帅
王俊和
闫帅帅
LIANG Baoyan ZHANG Wangxi WANG Yanzhi XU Shishuai WANG Junhe YAN Shuaishua(School of Materials and Chemical Engineering Zhongyuan University of Technology, Zhengzhou 450007, Chin)
出处
《中国陶瓷》
CAS
CSCD
北大核心
2016年第9期65-68,共4页
China Ceramics
基金
郑州市国际科技合作与交流项目(153PGJHZ209)
河南省教育厅重点项目(13A430132
151RTSTHN004)
河南省教育厅自然科学研究计划项目资助(12A430024
13A430128
14A430007)
河南省基础与前沿技术研究计划(132300410164)
河南省省院科技合作项目(122106000051
142106000193)
河南省科技开放合作项目(142106000051)
郑州市人才引育项目(141PRCYY514)
