摘要
目的：建立安宫牛黄丸质量控制方法。方法：运用薄层色谱法对栀子、郁金进行定性,高效液相色谱法对安宫牛黄丸中栀子苷进行定量。结果：薄层色谱图谱中能有效检出栀子、郁金。栀子苷在0.02~0.1mg/m L,线性关系良好（r=0.9998）;平均回收率为99.26%,RSD为0.91%。结论：该法专属性强,简单易行,可作为安宫牛黄丸的质量控制方法。
Objective： To establish a quality control method for An＇gong Niuhuang Wan. Methods： Zhizi and Yujin were qualified by TLC; and geniposide in An＇gong Niuhuang Wan was quantified by HPLC. Results： Zhizi and Yujin could be detected by TLC. Geniposide during 0.02 ~ 0.1mg/m L shows a good linear relationship（r =0.9998）. The average recovery rate was 99.26%; RSD was 0.91%. Conclusion： This method is selective, simple, accurate and suitable for the quality control of An＇gong Niuhuang Wan.
出处
《中医临床研究》
2016年第28期29-31,共3页
Clinical Journal Of Chinese Medicine
