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Electrochemical co-deposition of reduced graphene oxide-gold nanocomposite on an ITO substrate and its application in the detection of dopamine 被引量:2

Electrochemical co-deposition of reduced graphene oxide-gold nanocomposite on an ITO substrate and its application in the detection of dopamine
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摘要 The simultaneous deposition of rGO and gold nano structures has been achieved by electrodeposition from mixed solutions containing graphene oxide(GO)and a gold precursor.Scanning electron microscope(SEM),Raman spectroscopy and atomic force microscopy(AFM)have been employed to reveal the morphology,uniformity and practical stability of the nanocomposite films on the indium tin oxide(ITO)substrate.The AFM data showed heights of tens of nanometers of the nanocomposite,suggesting that multilayers of rGO with gold nanoparticles had been formed as a result of the electrochemical co-deposition.Differential pulse voltammetry(DPV),as a widely used analytical technique,has been carried out on the rGO-Au/ITO electrode for the quantitative detection of dopamine(DA).The detection limit(S/N=3)for the determination of DA was evaluated as 0.6μM. The simultaneous deposition of rGO and gold nano structures has been achieved by electrodeposition from mixed solutions containing graphene oxide(GO)and a gold precursor.Scanning electron microscope(SEM),Raman spectroscopy and atomic force microscopy(AFM)have been employed to reveal the morphology,uniformity and practical stability of the nanocomposite films on the indium tin oxide(ITO)substrate.The AFM data showed heights of tens of nanometers of the nanocomposite,suggesting that multilayers of rGO with gold nanoparticles had been formed as a result of the electrochemical co-deposition.Differential pulse voltammetry(DPV),as a widely used analytical technique,has been carried out on the rGO-Au/ITO electrode for the quantitative detection of dopamine(DA).The detection limit(S/N=3)for the determination of DA was evaluated as 0.6μM.
出处 《Science China Chemistry》 SCIE EI CAS CSCD 2017年第1期151-156,共6页 中国科学(化学英文版)
基金 the National Natural Science Foundation of China(21173048,21073038)
关键词 ELECTRODEPOSITION graphene GOLD nanocomposite films ITO电极 电化学还原 氧化石墨 纳米金 多巴胺 化学共沉积 扫描电子显微镜 铟锡氧化物
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