摘要
The MoS2 microspheres with high specific surface area assembled by ultrathin nanosheets have been successfully synthesized by a facile and environmentally friendly reaction in a closed reactor at moderate temperatures.The solid-state assembly was realized by a simple calcination process,and the annealing temperature played a key role in the formation of the final microspheres.The influences of reaction temperature were carefully investigated.A possible formation mechanism about the solid-state assembly was proposed based on the experimental results.
The MoS2 microspheres with high specific surface area assembled by ultrathin nanosheets have been successfully synthesized by a facile and environmentally friendly reaction in a closed reactor at moderate temperatures.The solid-state assembly was realized by a simple calcination process,and the annealing temperature played a key role in the formation of the final microspheres.The influences of reaction temperature were carefully investigated.A possible formation mechanism about the solid-state assembly was proposed based on the experimental results.
基金
Funded by the National Natural Science Foundation of China(Nos.51275213,51302112)
the Jiangsu Colleges and Universities Nature Science Foundation(No.14KJB430009)
the Jiangsu Industry-University-Research Joint Innovation Foundation(Nos.BY213065-05,Y213065-06)
Jiangsu Graduate Student Innovation Project(No.CXZZ13_0669)
