摘要
以乙烯基甲醚和三氯乙酰氯为原料,经加成-消除反应、加成反应、卤仿反应及消除反应合成标题化合物,总收率为56.5%。该合成方法原料廉价且简单易得、反应条件温和、操作简单安全,有工业产业化应用前景。
A new synthetic method of methyl 3-methoxyacrylate was established in this work.Methyl 3-methoxyacrylate was obtained from methyl vinyl ether and trichloroacetyl chloride as starting material via addition-elimination reaction,elimination reaction,haloform reaction and elimination reaction.The total yield is 56.5%.In this method,material is cheap and easily available,reaction conditions are mild,the operation is simple and safe,and it has the prospect of industrial application.
出处
《化学试剂》
CAS
北大核心
2017年第4期421-424,共4页
Chemical Reagents
