摘要
Bamboo shoot shell（BSS）,a by-product from bamboo shoot processing industries,is a natural resource of cellulose. In this study,high-pressure homogenization assisted with acidolysis treatment was employed to produce BSS cellulose nanofiber（CNF）,and the structure was characterized by powder X-ray diffraction（XRD）,Fourier-transform infrared（FT-IR） spectroscopy,atomic force microscopy（AFM）,high resolution transmission electron microscopy（HTTEM）,thermogravimetric analysis（TGA）,and ^13 C nuclear magnetic resonance（NMR）. Moreover,the structure and properties of CNF were compared with those of BSS insoluble dietary fiber（IDF）. The results showed that CNF was in the form of a grid-like micro fiber,and its particle size was obviously reduced,while the crystallinity,thermal stability and solubility were increased. The results indicated that high-pressure homogenization assisted with acidolysis treatment was an effective method to prepare the BSS CNF,which could be a promising biopolymer reinforced material.
Bamboo shoot shell（BSS）,a by-product from bamboo shoot processing industries,is a natural resource of cellulose. In this study,high-pressure homogenization assisted with acidolysis treatment was employed to produce BSS cellulose nanofiber（CNF）,and the structure was characterized by powder X-ray diffraction（XRD）,Fourier-transform infrared（FT-IR） spectroscopy,atomic force microscopy（AFM）,high resolution transmission electron microscopy（HTTEM）,thermogravimetric analysis（TGA）,and ^13 C nuclear magnetic resonance（NMR）. Moreover,the structure and properties of CNF were compared with those of BSS insoluble dietary fiber（IDF）. The results showed that CNF was in the form of a grid-like micro fiber,and its particle size was obviously reduced,while the crystallinity,thermal stability and solubility were increased. The results indicated that high-pressure homogenization assisted with acidolysis treatment was an effective method to prepare the BSS CNF,which could be a promising biopolymer reinforced material.
