摘要
利用固体碱为催化剂,采用一步法合成9-芴甲醇,考察了主要影响因素对产品收率的影响。甲苯和环己烷混合溶剂对粗品提纯能使产品含量达到95%以上,收率达到40%以上。
Solid base was used as catalyst for synthesizing 9-fluorene methanol by ＂ one step method＂. The effect of main factors to the yield of product was studied. The mixture solvent of toluene and cyclohexane can improve the purity of the product to 95% and higher, and the yield of the product to 40% and higher.
出处
《燃料与化工》
2017年第3期38-40,44,共4页
Fuel & Chemical Processes
关键词
芴
9-芴甲醇
固体碱
合成
Fluorene
9-fluorene methanol
Solid base
Synthesis
