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高效液相色谱法测定健阳片中淫羊藿苷和甘草酸的含量 被引量:3

Determination of Icariin and glycyrrhizic acid in Jianyang tablets by HPLC
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摘要 目的:建立健阳片的质量控制方法。方法:采用高效液相色谱法(HPLC法)测定健阳片中淫羊藿苷、甘草酸的含量。结果:淫羊藿苷在0.1288~2.576μg范围内线性关系良好,加样回收率为98.35%,RSD为1.35%;甘草酸在0.1646~3.292μg范围内线性关系良好,加样回收率为98.56%,RSD为0.71%。结论:本方法简便,重复性好,可用于该制剂的质量控制。 Objective: To establish a method for quality control of Jianyang tablets. Methods: The contents of icariin and glycyrrhizic acid were deter-minated by HPLC. Results: The linear range of icariin was 0.1288 -2.576μg,the average recovery of icariin was 98.35% and relative standard de-viation(RSD)was 1.35%(n=6).The linear range of glycyrrhizic acid was 0.1646-3.292μg,the average recovery of glycyrrhizic acid was 98.56% and relative standard deviation(RSD)was 0.71%(n=6). Conclusion: The methods is simple and repeatable, It can be used for quality control of Jianyang tablets.
作者 王钧
出处 《内蒙古中医药》 2017年第9期142-143,共2页 Inner Mongolia Journal of Traditional Chinese Medicine
关键词 淫羊藿苷 甘草酸 健阳片 HPLC Icariin glycyrrhizic acid Jianyang tablets HPLC
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