摘要
Amorphous ribbons with（Nd_（0.75）Pr_（0.25））_（9.5）Fe_（76）X_4B_（10.5）（X=Nb, Zr） nominal composition were annealed by conventional and microwave-assisted annealing furnaces, respectively. The thermal decomposition process, structure and magnetic properties of products were characterized by a thermal differential scanning calorimeter（DSC）, X-ray diffraction（XRD） and a vibrating sample magnetometer（VSM）. The addition of Nb and Zr increased the glass-forming ability（GFA） of as-spun ribbons. The proportion of Nd_2Fe_（14）B and α-Fe could be adjusted with power from 800 to 2000 W in microwave annealing process, during which the well-coupling between the soft and hard magnetic phase and higher coercivity reached up to 780.2 and 815.4 kA/m for（Nb,Zr）-doped alloys. The best magnetic properties of ribbons could be obtained by annealing at 650 oC for 10 min under the microwave power of 2000 W.
Amorphous ribbons with（Nd_（0.75）Pr_（0.25））_（9.5）Fe_（76）X_4B_（10.5）（X=Nb, Zr） nominal composition were annealed by conventional and microwave-assisted annealing furnaces, respectively. The thermal decomposition process, structure and magnetic properties of products were characterized by a thermal differential scanning calorimeter（DSC）, X-ray diffraction（XRD） and a vibrating sample magnetometer（VSM）. The addition of Nb and Zr increased the glass-forming ability（GFA） of as-spun ribbons. The proportion of Nd_2Fe_（14）B and α-Fe could be adjusted with power from 800 to 2000 W in microwave annealing process, during which the well-coupling between the soft and hard magnetic phase and higher coercivity reached up to 780.2 and 815.4 kA/m for（Nb,Zr）-doped alloys. The best magnetic properties of ribbons could be obtained by annealing at 650 oC for 10 min under the microwave power of 2000 W.
基金
Project supported by State Key Laboratory for Advanced Metals and Materials of China(2013-Z02)
the Project of Shanghai Science and Technology Committee(16090503600)
