摘要
Billets of Mg-9Al-3Zn-1Mn-6Ca-2Nd alloy were produced by spray-deposition（the Osprey process）.Effect of rolling deformation（T = 350？C, ε = 5%, 10%, and 15%, respectively） on microstructure and texture evolution of the Mg-9Al-3Zn-1Mn-6Ca-2Nd alloy was investigated by scanning electron microscopy（SEM）, transmission electron microscopy（TEM） and X-ray diffraction（XRD）. Results show that at pass reduction of ε = 5%, 10% and 15% at 350？C respectively, Mg-Nd-Zn typed 24R-LPSO structure was formed in（Ca, Nd）Al2phase（C15 Laves phase）. With the increase in pass reduction（i.e. 5%, 10% and 15%）, the texture pole density level of basal texture（0002） changed little and pyramidal texture（10 1ˉ3） were increased.In contrast, those of prismatic texture {101ˉ0} 〈11 2ˉ0〉 were increased initially and followed by a reduction, indicating texture randomization in the grain-refined Mg alloy. The combined contribution of LPSO phase and C15 phase was key to randomize the texture of the grain-refined Mg alloy. It was noted that the microcosmic plastic deformation of LPSO phase and nanometer-sized dispersed C15 phase impeded dislocation movement, led to dislocation tangles, and facilitated recrystallization.
Billets of Mg-9Al-3Zn-1Mn-6Ca-2Nd alloy were produced by spray-deposition（the Osprey process）.Effect of rolling deformation（T = 350？C, ε = 5%, 10%, and 15%, respectively） on microstructure and texture evolution of the Mg-9Al-3Zn-1Mn-6Ca-2Nd alloy was investigated by scanning electron microscopy（SEM）, transmission electron microscopy（TEM） and X-ray diffraction（XRD）. Results show that at pass reduction of ε = 5%, 10% and 15% at 350？C respectively, Mg-Nd-Zn typed 24R-LPSO structure was formed in（Ca, Nd）Al2phase（C15 Laves phase）. With the increase in pass reduction（i.e. 5%, 10% and 15%）, the texture pole density level of basal texture（0002） changed little and pyramidal texture（10 1ˉ3） were increased.In contrast, those of prismatic texture {101ˉ0} 〈11 2ˉ0〉 were increased initially and followed by a reduction, indicating texture randomization in the grain-refined Mg alloy. The combined contribution of LPSO phase and C15 phase was key to randomize the texture of the grain-refined Mg alloy. It was noted that the microcosmic plastic deformation of LPSO phase and nanometer-sized dispersed C15 phase impeded dislocation movement, led to dislocation tangles, and facilitated recrystallization.
作者
Zhenliang Li
Fei Liu
Aiping Yuan
Baoyu Duan
Yiming Li
Xiaowei Li
Zhenliang Li Fei Liu Aiping Yuan Baoyu Duan Yiming Li Xiaowei Li(School of Materials and Metallurgy, Inner Mongolia University of Science ＆ Technology, Baotou 014010, China Analysis and Test Center, Inner Mongolia University of Science ＆ Technology, Baotou 014010, China)
基金
financial support by the National Natural Science Foundation of China (No. 51364032)
