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静电纺丝技术制备Zn(HDz)_2/PVA纳米带与表征

Preparation and Characterization of Zn(HDz)_2/PVA Nanobelts by Electrospinning Technique
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摘要 采用静电纺丝技术制备Zn(HDz)_2/PVA复合纳米带,用XRD、SEM、FTIR、UV-Vis等技术对样品进行了表征。XRD分析表明,该复合纳米带为无定型的。FTIR分析表明,所制备的Zn(HDz)_2/PVA复合纳米带的主要成分为聚乙烯醇(PVA)。通过SEM照片,可以看出Zn(HDz)_2/PVA复合纳米带表面光滑,尺寸均一,纳米带的长度可达到1cm,且宽厚比较大,厚度约为100~200nm,平均宽度约为1.8μm。UV-Vis分析表明,Zn(HDz)_2/PVA复合纳米带具有良好的光致变色性质。 Zn(HDz)2/PVA composite nanobelts were prepared by electrospinning technique. The samples were characterized by X-ray diffratometry(XRD), scanning electron microscopy(SEM), Fourier transform infrared spectrometry(FTIR) and UV-visible spectrophotometer(UV-Vis). XRD results showed that Zn(HDz)2 /PVA composite nanobelts were amorphous in structure. FTIR analysis manifested the Zn(HDz)2/PVA composite nanobelts major constituent were PVA. SEM analysis indicated the width of the Zn(HDz)2/PVA composite nanobelts were in narrow range, the average width of composite nanobelts were 1.2~1.4μm, the length of composite nanobelts were 1cm and the photochromism aspect. UV-Vis analysis indicated the Zn(HDz)2/PVA composite nanobelts had good photochromic properties.
出处 《化工技术与开发》 CAS 2017年第9期1-4,共4页 Technology & Development of Chemical Industry
基金 2016国家级大学生创新创业训练项目(201611396024)
关键词 静电纺丝技术 纳米带 Zn(HDz)2/PVA 光致变色 electrospinning nanobelts Zn(HDz)2/PVA photochromism
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