摘要
目的:建立五加皮中活性成分紫丁香苷的最佳提取工艺。方法:通过溶剂回流、超声提取法以及索氏提取法,分别控制反应时间、液料比、溶剂等单因素实验考察其对五加皮中活性成分提取率的影响。结果:五加皮中草药活性成分最佳提取工艺为:丙酮为溶剂、液料比6︰1、回流6小时提取率最高。结论:该方法简单易行,灵敏可靠,经济适用,重复性好,为五加皮中草药中提取活性成分紫丁香苷的提供了一个简单易行的方法。
Objective To establish a determination method of extracting process from cortex acanthopanacis by HPLC. Methods Through altering extraction process conditions by single factor test to investigate the extraction effect of active components in cortex acanthopanacis. Results The optimum process conditions are reflux extraction with acetone, liquid-solid ratio of 6 : 1, reflux, 6 hours. Conclusion: Methodology examination indicated this optimized process is simple, stable, feasible and reliable, suitable for mass production of the active component syringoside.
作者
王秀皊
刘玉
曹乐
薛洪宝
梁丽丽
Wang XiuLing Liu Yu Cao Le Xue Hongbao Liang Lili(Department of Pharmaceutical Engineering, Bengbu Medical College, Bengbu 233030, Chin)
出处
《广东化工》
CAS
2017年第20期32-33,共2页
Guangdong Chemical Industry
基金
国家级大学生创新创业项目(201510367004)