摘要
Pd (p-CH3C6H4SC4H9)2Cl2C(22)H(32)CL2S2Pd , MR= 537. 92, space group P21/c, a=10. 336(2) , b=8. 657(1) ,c=14. 452(2) A, β=105. 19(1)°, V = 1247. 9(3) A3, Z=2 , Dc= 1. 43 g/cm￣(-3), MoKα radiation,μ=11. 16 cm-1,F(000) = 552 , R= 0. 030 for 2417 reflections with I】3a(Ⅰ) .Pd (Ⅱ) is coordinated by two chloride atoms and two sulfur atoms of organic ligands, forming a transsquare planar with Pd-S of 2. 316(1) and Pd-Cl of 2. 303(1) A.
Pd (p-CH3C6H4SC4H9)2Cl2C(22)H(32)CL2S2Pd , MR= 537. 92, space group P21/c, a=10. 336(2) , b=8. 657(1) ,c=14. 452(2) A, β=105. 19(1)°, V = 1247. 9(3) A3, Z=2 , Dc= 1. 43 g/cm￣(-3), MoKα radiation,μ=11. 16 cm-1,F(000) = 552 , R= 0. 030 for 2417 reflections with I>3a(Ⅰ) .Pd (Ⅱ) is coordinated by two chloride atoms and two sulfur atoms of organic ligands, forming a transsquare planar with Pd-S of 2. 316(1) and Pd-Cl of 2. 303(1) A.
