摘要
建立了气相色谱法测定土壤、沉积物中测定沸点在175℃~525℃范围内的烃类,包括C_(10)H_(22)~C_(40)H_(82)的正构烷烃以及异构烷烃、环烷烃、烷基苯、烷基萘和多环芳烃。当取样量为20.0g时,土壤中可萃取石油烃的方法检出限为2.750 mg/kg,测定下限为8.26 mg/kg。曲线方程为y=45.556x,相关系数为0.9970,加标回收率高相对标准偏差为0.2。
A gas chromatographic is established for the determination of hydrocarbons in the soil and sediments with boiling points in the range of 175-525 ℃,including normal alkanes of C10H22-C40H82andisomerization alkane,cyclanes and alkyl benzenes,alkyl naphthalene and polycyclic aromatic hydrocarbons.When the sample size is 20.0 g,the method of extracting petroleum hydrocarbon in soil is 2.750 mg/kg and the lower limit is 8.26 mg/kg.The curve equation is y=45.556 x;the correlation coefficient is 0.9970 and the standard deviation of high standard deviation is0.2.
作者
于雅东
Yu Yadong(College of Environmental Science and Engineering ,Qilu University of Technology （Shandong Academy of Sciences）,Jinan, Shandong, 250300, Chin)
出处
《绿色科技》
2018年第8期99-100,共2页
Journal of Green Science and Technology
关键词
气相色谱
石油烃
快速溶剂萃取
gas chromatography
petroleum hydrocarbon
rapid solvent extraction
