摘要
阳极铜样品用(1+2)硝酸溶解后,定容500 mL,分取50 mL,浓缩体积约10 mL,硫氰酸钾浓度(400g/L),用Na_2S_2O_3标准溶液滴定。实验证明,该方法操作简便、准确度和精密度都能满足生产分析要求,可以应用于阳极铜中铜的检测分析过程中。
Anode copper sample was dissolved by nitric acid(1+2)、and diluted to 500 mL,taken 50 mL and concentrated to 10 mL,potassium thiocyanate concentration(400 g/L)and titration with Na_2S_2O_3 standard solution.Experimental results show that the method is simple,accurate and precise,and can be applied to the detection and analysis of copper in anode copper.
作者
吕彦玲
LU Yan-ling(Baiyin Non-ferrous Group Co. Ltd., Baiyin 730900, Chin)
出处
《甘肃冶金》
2018年第3期86-87,共2页
Gansu Metallurgy
关键词
阳极铜
硫氰酸钾
碘量法
anode copper
potassium thiocyanate
iodine quantity method