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Controlled synthesis of magnetic carbon nanoparticles via glycerol/ferrocene co-pyrolysis with magnetic induction

Controlled synthesis of magnetic carbon nanoparticles via glycerol/ferrocene co-pyrolysis with magnetic induction
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摘要 We performed a controlled synthesis of magnetic carbon nanoparticles （M-CNPs） via co-pyrolysis of glycerol and ferrocene with magnetic induction. The morphology of the synthesized M-CNPs was confirmed by transmission electron microscopy, and thermogravimetric analysis was used to analyze the carbon and Fe contents. M-CNPs that responded to magnetic stimulation were also examined with an AC-magnetic susceptibility analyzer. Our investigations on the influence of synthesis temperature in the range 700-1000℃ suggested that for an initial glycerol to ferrocene weight ratio of 3：1 and a temperature of 800 ℃ gave the highest yield of M-CNPs. Comparing the synthesis with and without magnetic induction, the controlled synthesis under the influence of magnetic induction shows promise as a method for producing high quality M-CNPs in high yields. We performed a controlled synthesis of magnetic carbon nanoparticles （M-CNPs） via co-pyrolysis of glycerol and ferrocene with magnetic induction. The morphology of the synthesized M-CNPs was confirmed by transmission electron microscopy, and thermogravimetric analysis was used to analyze the carbon and Fe contents. M-CNPs that responded to magnetic stimulation were also examined with an AC-magnetic susceptibility analyzer. Our investigations on the influence of synthesis temperature in the range 700-1000℃ suggested that for an initial glycerol to ferrocene weight ratio of 3：1 and a temperature of 800 ℃ gave the highest yield of M-CNPs. Comparing the synthesis with and without magnetic induction, the controlled synthesis under the influence of magnetic induction shows promise as a method for producing high quality M-CNPs in high yields.
作者 Konrat Kerdnawee Noriaki Sano Hajime Tamon Tawatchai Charinpanitkul
机构地区 Center of Excellence in Particle Technology Department of Chemical Engineering
出处 《Particuology》 SCIE EI CAS CSCD 2018年第2期9-16,共8页 颗粒学报（英文版）
关键词 Carbon nanoparticle Glycerol Co-pyrolysis Magnetic induction Carbon nanoparticle Glycerol Co-pyrolysis Magnetic induction
分类号 TQ133.1 [化学工程—无机化工] TG139.8 [一般工业技术—材料科学与工程]
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Particuology
2018年 第2期

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